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(6)ๅถๅคFmoc-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-WangResin (6) Preparation of Fmoc-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-WangResin ๅจๆญฅ้ชค(5)็Fmoc-Asp(otBu)-Ala-Gly-Leu-Val-WangResinไธญ๏ผๅ ๅ ฅ่ฑๅธฝ่ฏๅ(20๏ผ ๅๅถ็DMFๆบถๆถฒ)๏ผๅธธๆธฉๅๅบ5ๅ้๏ผๆฝๅนฒ๏ผ้ๆฐๅ ๅ ฅ่ฑๅธฝๅๅธธๆธฉๅๅบ20ๅ้๏ผ็จๅผไธ้ๆดๆถค3ๆฌก๏ผDMFๆดๆถค3ๆฌก๏ผ้่ธ่ฟ็DMFๆดๆถค2ๆฌก๏ผๆฝๅนฒ๏ผๅ ๅ ฅFmoc-Asp(otBu)-OH1.1g๏ผDIEA0.4ml๏ผTBTU0.56g๏ผHOBT0.2g๏ผDMF10mlๅธธๆธฉๅๅบ1.5ๅฐๆถ๏ผ็จ็็ฉบๆณตๆฝๅนฒ๏ผ็จๅผไธ้ๆดๆถค3ๆฌก๏ผDMFๆดๆถค3ๆฌก๏ผ้่ธ่ฟ็DMFๆดๆถค2ๆฌก๏ผๆฝๅนฒ๏ผ่ทๅพFmoc-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-WangResin๏ผ In the Fmoc-Asp(otBu)-Ala-Gly-Leu-Val-WangResin in step (5), add decapping reagent (20% piperidine in DMF solution), react at room temperature for 5 minutes, drain, and add decapping reagent at normal temperature React for 20 minutes, wash with isopropanol for 3 times, DMF for 3 times, DMF for redistilled for 2 times, drain, add Fmoc-Asp(otBu)-OH1.1g, DIEA0.4ml, TBTU0.56g, HOBT0 .2g, DMF10ml normal temperature reaction for 1.5 hours, drained with a vacuum pump, washed 3 times with isopropanol, washed 3 times with DMF, washed 2 times with DMF evaporated, and dried to obtain Fmoc-Asp(otBu)-Asp(otBu )-Ala-Gly-Leu-Val-WangResin
Hair Growth
Size:240 Caps
GMP-manufactured in the USA
Ships within 48 hours ยท Estimated delivery Oct 15 - Oct 20
US$40
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