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melanotan 2 org II (MT-2) medical #knowledge #π§ββοΈπ©ΊβοΈππππ₯Ί
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melanotan 2 org II (MT-2) medical #knowledge #π§ββοΈπ©ΊβοΈππππ₯Ί
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melanotan 2 org II (MT-2) medical #knowledge #π§ββοΈπ©ΊβοΈππππ₯Ί
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melanotan 2 org II (MT-2) medical #knowledge #π§ββοΈπ©ΊβοΈππππ₯Ί
medical #knowledge #π§ββοΈπ©ΊβοΈππππ₯Ί
(6)εΆε€Fmoc-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-WangResin (6) Preparation of Fmoc-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-WangResin ε¨ζ₯ιͺ€(5)ηFmoc-Asp(otBu)-Ala-Gly-Leu-Val-WangResinδΈοΌε ε ₯θ±εΈ½θ―ε(20οΌ εεΆηDMFζΊΆζΆ²)οΌεΈΈζΈ©εεΊ5ειοΌζ½εΉ²οΌιζ°ε ε ₯θ±εΈ½εεΈΈζΈ©εεΊ20ειοΌη¨εΌδΈιζ΄ζΆ€3欑οΌDMFζ΄ζΆ€3欑οΌιθΈθΏηDMFζ΄ζΆ€2欑οΌζ½εΉ²οΌε ε ₯Fmoc-Asp(otBu)-OH1.1gοΌDIEA0.4mlοΌTBTU0.56gοΌHOBT0.2gοΌDMF10mlεΈΈζΈ©εεΊ1.5ε°ζΆοΌη¨η空泡ζ½εΉ²οΌη¨εΌδΈιζ΄ζΆ€3欑οΌDMFζ΄ζΆ€3欑οΌιθΈθΏηDMFζ΄ζΆ€2欑οΌζ½εΉ²οΌθ·εΎFmoc-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-WangResinοΌ In the Fmoc-Asp(otBu)-Ala-Gly-Leu-Val-WangResin in step (5), add decapping reagent (20% piperidine in DMF solution), react at room temperature for 5 minutes, drain, and add decapping reagent at normal temperature React for 20 minutes, wash with isopropanol for 3 times, DMF for 3 times, DMF for redistilled for 2 times, drain, add Fmoc-Asp(otBu)-OH1.1g, DIEA0.4ml, TBTU0.56g, HOBT0 .2g, DMF10ml normal temperature reaction for 1.5 hours, drained with a vacuum pump, washed 3 times with isopropanol, washed 3 times with DMF, washed 2 times with DMF evaporated, and dried to obtain Fmoc-Asp(otBu)-Asp(otBu )-Ala-Gly-Leu-Val-WangResin
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Size:240 Caps
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melanotan 2 org II (MT-2) medical #knowledge #π§ββοΈπ©ΊβοΈππππ₯Ί
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